Air sampling

Atmospheric air
Industrial emissions
Occupational air
Indoor air

Sampling of atmospheric air

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№ № RD Name of the characteristic being defined What to sample for Sampling speed Sampling time Shelf life Note
1 GOST 17.2.4-05 suspended substances (dust) AFA-VP filter 75 dm3/min At the end of sampling the total volume of air passed is recorded. - -
2 RD 52.04.792-14 (FR.1.31.2015.19877) Nitrogen dioxide two series-connected ST 412 and a desiccant and ST-oxidizer located between them 0, 5dm3/min 30 10 days When determining single concentration of nitrogen oxide and nitrogen dioxide: attach system consisting of two series-connected ST 412 and located between them along the air flow: a column filled with 10 cm of desiccant, and ST-oxidizer. When sampling, the column and sorption tubes should be fixed vertically with a layer of sorbent down. Air must pass from the bottom up.All connections are made with rubber couplings end-to-end.
When determining the daily concentration of nitrogen oxide and nitrogen dioxide from a single sample, the test air is aspirated discretely, twelve times in 1 day for 20 minutes at regular intervals with a flow rate of 0.3 dm/min through a system consisting of two series-connected ST 412, prepared for selection and located between them along the air flow: a column filled with 100 cm of desiccant, and ST-oxidizer. When sampling columns and sorption tubes should be strengthened in a vertical position with a layer of sorbent down. Air must pass from the bottom up. All connections are made with rubber couplings end-to-end.
Sampling can be carried out at the temperature of the air passing through the sorption tube from minus 10°C to 40°C. In the absence of sorption tubes ST 412 instead of each of them, the scheme includes two sorption tubes ST 212.
Nitrogen oxide
3 RD 52.04.791-14 (FR.1.31.2015.19887) Ammonia sorption tube 2.0 dm3 / min 20 5 days Sorption tube should be fixed vertically with a layer of sorbent down. In order to delay the aerosol of ammonium salts during sampling, a filter holder with an AFA-VP-10 filter is connected to the sorption tube at the air inlet. All connecting tubes must be made of fluoropolymer and connected end-to-end with clean (washed and dried) rubber couplings. Care must be taken to ensure that the inner surface of the connecting tubes is dry to avoid ammonia sorption in them.
Air must pass from the bottom up. Sampling can be carried out at the temperature of the air passing through the sorption tube from 0°C to 40°C.
4 MUK 4.1.596-96 Ammonium sulphate (as ammonium ion) AFA or " Sinyaya lenta" 20 dm3/min 10-20 7 days -
Ammonium persulphate (as ammonium ion) 1 day
5 RD 52.04.797-14 (FR.1.31.2015.19878) Hydrogen fluoride (hydrofluoride) sorption tube 3 dm3/min 20 7 days When sampling, sorption tube should be strengthened in a vertical position with a layer of sorbent down. Air must go up from the bottom. Sampling can be performed at the temperature of the analyzed air from minus 10°C to 40°C. A filter holder with a filter for capturing solid fluorides and other aerosols is installed in front of the sorption tube using a polyethylene corner. Sorption tube, corner and filter holder must be connected end-to-end, so that there is no contact of air with the rubber. When determining daily concentrations, at least four single samples are taken at regular intervals.
6 RD 52.04.793-14 (FR.1.31.2015.19882) Hydrogen fluoride (hydrofluoride) AFA-PV-10 filter and sorption tube 4 dm3/min 20 10 days Filter holder with the filter and the sorption tube are connected by a rubber coupling end-to-end. Sorption tube should be fixed vertically with a layer of sorbent down. Air must flow from the bottom up. Sampling can be performed at the temperature of the analyzed air passing through the sorption tube, from 0°C to 40°C.
At the expected concentrations of hydrogen chloride from 5 to 10 MPC, the volume air flow should be reduced to 2 dm/min. When determining daily concentration, at least four single samples are taken at regular intervals.
7 RD 52.04.795-14 (FR.1.31.2015.19886) Hydrogen sulfide (dihydrosulfide) sorption tube 4 dm3/min 20 2-3 days When selecting sorption tube should be strengthened in a vertical position with a layer of sorbent down and protected from light by a screen made of black paper or foil.
8 RD 52.04.794-14 (FR.1.31.2015.19884) Sulfur dioxide Richter absorbers 2,5 dm3/min 20 7 days In case of high expected mass concentrations of sulfur dioxide, air consumption can be reduced to 0.5 dm/min. When determining daily concentrations, at least four single samples are taken at regular intervals. Sampling can be carried out at the temperature of the analyzed air from 0°C to 40°C. Samples must be protected from direct sunlight during sampling and storage.
9 RD 52.04.831-15 (FR.1.31.2016.23390) Soot (carbon-containing aerosol) AFA-HP-10 AFA-VP10 20 дм3/мин 30 unlimited Sampling is carried out on the windward side at a height of 1.5 m from the ground surface.
10 RD 52.04.798-14 (FR.1.31.2015.19880) chlorine Richter absorber 0,5 dm3/min 20 3 days When determining daily concentration, at least four single samples are taken at regular intervals.
11 MUK 4.1.615-96 Potassium chloride AFA-VP-20 10 dm3/min 12.5 1 month -
12 MUK 4.1.1044 a-01 Dimethyamine at the same time on 2 sorption tubes (sorbent Chromosorb 106 or 103) 0,2 dm3/min 10 3 days Air is aspirated through a pre-cooled to 0°C outlet of a sorption tube.
Diethylamines
Propylamines
Triethylamines
Ethylamines
Dimethylformamide
13 GOST R ISO 16017-1 Acetonitrile sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min Depending on the conditions 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
Acrylonitrile (prop-2-isonitrile)
Hexane
Heptane
Decane
Dodecane
Nonane
Octane
Aliphatic saturated hydrocarbons of the gasoline fraction C6-C12
Undecane
Acetone (propan-2-one)
Methylethyl ketone (Butanone)
Hexanon
Diacetone alcohol (4-hydroxy-4-methyl-2-pentanone)
Cyclohexanone
Benzene
Isopropylbenzene (Cumene)
Xylene (dimethylbenzene)
Pseudocumene (1,2,4-trimethylbenzene)
Styrene (ethenylbenzene)
Toluene (methylbenzene)
Ethylbenzene
Vinyl chloride (chloroethene)
Dichloromethane
1.1-dichloroethylene
Trichloroethane
Trichloroethylene
Carbon tetrachloride (tetrachloromethane)
Chlorobezene
Chloroform (trichloromethane)
Butanol
1.2-dichloroethane
GOST R ISO 16017-1 Isobutanol sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min Depending on the conditions 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
(2-methylpropan-1-ol)
Methanol (carbinol)
Amyl alcohol (pentanol)
Propyl alcohol (propan-1-ol)
Cyclohexanol (cyclohexyl alcohol)
Ethanol (ethyl alcohol)
Phenol (hydroxybenzene)
Butylacetate
Dibutylphthalate
Dimethylphthalate
Dimethylisophthalate
Diethylphthalate
Isobutylacetate
Methylacetate
Propylacetate
Vinylacetate (Ethenylacetate)
Ethylacrylate
Ethylacetate
14 MUK 4.1.629-96 Nitriles (C10-C16) Yavorovskaya absorption device 10 dm3/min 30 5 hours -
15 FR.1.31.2011.11272 (M-22) Butadiene (buta-1,3-diene) 2 series-connected (end-to-end) sorption concentrator tubes (TENAX sorbent) 0,3 dm3/min 30 2 days in refrigerator When determining surface concentration of a substance in the atmosphere, samples are taken at an altitude of 1.0 - 3.5 m from the earth's surface.Each sample is taken on 2 sequentially connected (end-to-end) sorption tubes installed vertically, with the inlet opening down.At expected mass concentrations not exceeding 1 mg/m3, sampling is performed with a volume flow rate of 0.3 dm3/min for 30 minutes. If the expected mass concentrations exceed 1 mg/m3, several samples are taken (2 - 3) with a lower volume flow rate during this time period.
Benzaldehyde
Methylacetate
Isopropyl acetate (1-methyethyl acetate)
n-propylacetate
isobutylacetate
N-Butylacetate
N-Amylacetate
Isoprene
N-Hexanol
2-Ethylhexanol
Octan-1-ol (n-oktyl alcohol)
Benzyl alcohol (benzyl carbinol)
Propionic acid
Pentanoic acid (valeric)
Hexanoic acid (capronic)
2-ethoxyethyl ether of acetic acid
FR.1.31.2011.11272 (M-22) Methylcellosolve (2-methoxyethanol) 2 series-connected (end-to-end) sorption concentrator tubes (TENAX sorbent) 0,3 dm3/min 30 2 days in refrigerator When determining surface concentration of a substance in the atmosphere, samples are taken at an altitude of 1.0 - 3.5 m from the earth's surface.Each sample is taken on 2 sequentially connected (end-to-end) sorption tubes installed vertically, with the inlet opening down.At expected mass concentrations not exceeding 1 mg/m3, sampling is performed with a volume flow rate of 0.3 dm3/min for 30 minutes. If the expected mass concentrations exceed 1 mg/m3, several samples are taken (2 - 3) with a lower volume flow rate during this time period.
Isopropylalcohol (2-isopropoxyethanol)
Diphenyl ether
Butylcellosolve (2-butoxyethanol)
Durol (1,2,4,5-tetramethylbenzene)
1-methoxypropan-2-ol
1-ethoxypropan-2-ol
4-methylpentan-2-ol
Cyclohexane
Methylbutanoate
Ethylbutanoate
Methylpropionate
Ethylpropionate
Ethylene glycol (1,2-ethanediol)
Propylene glycol (1,2-propanediol)
16 PND F 13.1:2:3.23-98 (FR.1.31.2015. 20483) butenes (butene-1, butene-2, isobutene) syringes 7-10 times pumping the syringe - 5 hours -
Ethene (ethylene)
Propene (propylene)
C1-C5 (saturated hydrocarb.)
17 PND F 13.1:2:3.25-99 (FR.1.31.2015.20480) C2-C5 (unsaturated) (total); syringes 7-10 times pumping the syringe - 5 hours -
C1-C10 (saturated) (total)
Benzene
Toluene
Ethylbenzene
Xylols
Styrene
18 FR.1.31.2011.11269 (M-24) isocyanates and aromatic amines (aniline, n-nitroaniline, toluylenediisocyanate) sorption tubes 5 dm3/min 60 - Collect 2 sampling lines. In each line, there are 2 sequentially connected tubes installed vertically with the sorbent down.
19 PND F 13.1:2: 3.59-07 (FR.1.31.2013.16458) (M 01-05) aliphatic saturated hydrocarbons of a kerosene fraction C12-C19 disposable carbon type sampler 0.2-0.3 dm3/min 20-30 7 days in refrigerator -
20 MUK 4.1.1957-05 vinyl chloride at the same time on 2 sorption tubes (sorbent Chromosorb 104) 0,2 dm3/min 10 3 days in refrigerator Each air sample is simultaneously sampled into two sorption tubes using 2 samplers.Air is pumped through a narrow opening of the sorption tube, cooled by a refrigerator with ice to 0 °C.
Acetaldehyde
21 MUK 4.1.616-96 formic acid sorption tubes ST 212 5 dm3/min 20 10 days -
acetic acid
propionic acid
butanoic acid
pentanoic acid
hexanoic acid
22 PND F 13.1:3.68-09 (FR.1.31.2015.19226) Benzene Absorption device with a porous plate 0.5 dm/min. 20-30 3 days in refrigerator -
Xylene (dimethylbenzene)
23 MUK 4.1.632-96 Ethyltoluene Absorption device with a porous plate 0.5 dm/min. 30 1 month in a dark and cool place -
Propylbenzene
Pseudocumene (1,2,4-trimethylbenzene)
Naphthalene 2 series-connected Richter absorbers 3 dm3/min 25 To capture acetic acid vapors, a glass tube with a diameter of 2 cm and a length of 10 cm filled with potassium hydroxide is placed in front of the aspirator. After sampling, the ends of the absorption vessels are fixed with glass plugs. The shelf life of the sample in test tubes with ground-glass stoppers in a dark and cool place is 1 month.
24 MUK 4.1.619-96 Methylmercaptan sorption tube-concentrator (TENAX sorbent) 1,5 dm3/min 30 3 days in refrigerator -
Propylmercaptan
Butylmercaptan
A mixture of natural mercaptans
25 RD 52.04.799-2014 (FR.1.31.2015.19883) Phenol (hydroxybenzene) sorption tube ST212 or ST 412 5 dm3/min 30 2 days at a temperature of 18°C to 25°C in the dark -
26 MUK 4.1.1143-02 Tiametoxam filter "Sinyaya lenta" 4 dm3/min 5 in a freezer at a temperature of -12 °C for 30 days, in a refrigerator at 4-6 °C - for 7 days. -
27 PND F 13.1:2: 3.71-11 (FR.1.31.2015.21767) Aluminum AFA-VP; AFA-HP; AFA-HA 50 dm3 / min 20 1 month Sampling is carried out at a height of 1.5 meters from the earth surface, the filter holder should be oriented towards the wind flow.
Barium
Beryllium
Vanadium
Bismuth
Tungsten
Iron
Gallium
Cadmium
Cobalt
Silicon
Lithium
PND F 13.1:2: 3.71-11 (FR.1.31.2015.21767) Magnesium AFA-VP; AFA-HP; AFA-HA 50 dm3 / min 20 1 month Sampling is carried out at a height of 1.5 meters from the earth surface, the filter holder should be oriented towards the wind flow.
Manganese
Arsenic
Copper
Molybdenum
Silver
Nikel
Tin
Mercury
Lead
Selenium
Antimony
Titanium
Chromium
Zinc
28 RD 52.04.823-2015 (FR.1.31.2016.23399) formaldehyde Richter absorption device 2 dm3/min 30 5 days -

Sampling of industrial emissions

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№ № RD Name of the characteristic being defined What to sample for Sampling speed Sampling time Shelf life Note
1 GOST 33007 Dust content (mass content) AFA-VP filter 10-20 dm3/min - - -
2 MON F 13.1.33-02 (FR. 1. 31. 2014. 18977) Ammonia 2 sequentially connected absorbers with a porous plate 0,5 dm3/min - - -
3 M-20 (FR. 1. 31. 2011. 11274) Inorganic compounds of phosphorus (V) (in terms of diphosphorus pentoxide) Dual SATA-VP filter (glass sampling tube with the desired spout diameter) 20 dm3/min 20 3 days -
4 M-7 (FR. 1. 31. 2011. 11266) Aerosol of caustic alkalis ( Dual SATA-VP filter (glass sampling tube with the desired spout diameter) 20 dm3/min 20 3 days -
5 MON F 13.1.45-03 (FR. 1. 31. 2015. 19221) Hydrogen fluoride (hydrofluoride) 3 Richter absorbers connected in series (12-16) dm3/min - - To prevent the absorption of hydrogen fluoride by a rubber hose, the absorption devices, the sampling tube and the trap are connected end-to-end. Cartridges are pre-filled with fluoroplastic chips, and then a swab of fluorine fiber is inserted. For dry gases with a temperature of less than 80°C, use polyethylene cartridges, more than 80°C-fluoroplastic cartridges. When sampling hydrogen fluoride from wet gases, a heated cartridge is used. Preheating is used to prevent the absorption of hydrogen fluoride by moisture that condenses in the cartridge. Gas consumption in the selection of 0.5-2.5 DM/min and a vacuum of 3.3 to 26.6 kPa. The temperature inside the cartridge should be 160-180°C.
6 MON F 13.1.42-03 (FR. 1. 31. 2015. 19224) Hydrogen chloride (hydrochloride) 2 sequentially connected absorbers with a porous glass plate 1 dm3/min 10-30 1 day -
7 M-3 (FR. 1. 31. 2011. 11281) Sulfuric acid (aerosol) Dual AFA-VP filter or AFA-HP (glass sampling tube with the desired diameter of the spout) 20 dm3/min 20 2 days -
8 MON F 13.1.46-04 (FR. 1. 31. 2007. 03828) Sulfuric acid vapors and sulfur trioxide aerosols (in terms of sulfuric acid) Glass sampling cassette (0.5-2.0) dm3 / min - - -
9 MON F 13.1.34-02 (FR. 1. 31. 2007. 03824) Hydrogen sulfide (dihydrosulfide) 4 Richter absorbers connected in series 0,4 dm3/min 10-30 min 1 day (preservation of 0.001% R-rum routine: 5-7 days) At the end of the sampling, it is necessary to determine the final concentration of alkali in the absorption solution, which should be at least 2 mol/dm3. To do this, 1 cm3 of a solution of sodium hydroxide C(NaOH) = 5 mol/dm3 is titrated with a solution of hydrochloric acid C(Hcl) = 0.5 mol/dm3 in the presence of 1-2 drops of phenolphthalein until the pink color disappears within 1 minute. The volume of hydrochloric acid used for titration (V1) is recorded. To the colorless solution, add 1 drop of methylorange (yellow solution) and continue to titrate with a solution of hydrochloric acid until the transition from yellow to orange color. The volume of hydrochloric acid used for titration of the alkaline solution with methylorange is recorded.< br> the concentration of sodium hydroxide (mol / dm3) is calculated by the formula:
C(NaOH) = ((V1 - V2) * C(HCl))/V3
where V1 is the amount of hydrochloric acid used for titrating the alkaline solution sample with the indicator phenolphthalein, cm3;
V2 is the amount of hydrochloric acid used for titrating the alkaline solution sample with the indicator methylorangem, cm3;
C(HCl) is the mass concentration of hydrochloric acid,
C(HCl) = 0.5 mol/Dm3;
v3 - the volume of the alkaline solution sample selected for analysis, cm3.
If the final concentration of alkali after sampling is less than 2 mol / dm3, the sampling is repeated using an absorption solution with an alkali concentration of 8 mol/dm3.
after passing a portion of gas, the absorbers are disconnected from the system and the free processes are closed with plugs. Samples are analyzed on the day of selection or preserved with a 0.001 % solution of rutin (arabino-galactan) for 5-7 days.
Methylmercaptan (methanethiol)
10 FR.1.31.2001.00384 Carbon (soot) АФА-ВП-20, АФА-ВП-10 (1-St.40) dm3/min. 20 - -
11 MON F 13.1.50-06 (FR. 1. 31. 2015. 19220) Chlorine Zaitsev absorption device 0,25 dm3/min 20 1 day When sampling in direct light, the absorption device is wrapped in black paper
12 FR. 1. 31. 2011. 11265 (M-10) Acrylonitrile (propane-2-ison sorption tube-concentrator (TENAX sorbent) 10 dm3/min. 20 Can be stored in the refriger At least 3 samples (2 parallel ones in each).
acetaldehyde (acetic aldehyde, ethanal) 5 dm3/min Immediately placed in a chilled container and stored for no more than 2 days
Dichloromethane (Methylene chloride) 10 dm3/min. Can be stored in the refrigerator for 2 weeks
dichloroethane
Tetrachloroethylene (perchloroethylene)
Trichloroethylene (trichloroethene)
Carbon tetrachloride (tetrachloromethane)
Chloroform (trichloromethane)
Epichlorohydrin (chloromethyloxirane)
13 FR.1.31.2011.11272 (M-22) Butadiene (buta-1,3-diene) sorption tube-concentrator (TENAX sorbent) 0,1 dm3/min 20 7 days in refrigerator Make 1-3 consecutive sampling (2 parallel samples for each selection)
Benzaldehyde
Methylacetate
Isopropyl acetate (1-methyethyl acetate)
n-propylacetate
isobutylacetate
N-Butylacetate
N-Amylacetate
Isoprene
N-Hexanol
2-этилгексанол
octane-1-ол (н-октиловый спирт)
Бензиловый спирт (бензилкарбинол)
Пропионовая кислота
ФР.1.31.2011.11272 (М-22) Пентановая к-та (валериановая) sorption tube-concentrator (TENAX sorbent) 0,1 дм3/мин 20 7 дней в холодильнике Производят 1-3 последовательных отбора проб (по 2 параллельных пробы для каждого отбора)
Hexaneовая к-та (капроновая)
2-ethoxyethyl ether of acetic acid
Methylcellosolve (2-methoxyethanol)
Изопрпилцеллозольв (2-изопропоксиэтанол)
Дифениловый эфир
Butylcellosolve (2-butoxyethanol)
Durol (1,2,4,5-tetramethylbenzene)
1-methoxypropan-2-ol
1-ethoxypropan-2-ol
4-methylpentan-2-ol
Cyclohexane
Methylbutanoate
Ethylbutanoate
Methylpropionate
Ethylpropionate
Ethylene glycol (1,2-ethanediol)
Propylene glycol (1,2-propanediol)
14 PND F 13.1:2:3.23-98 (FR.1.31.2015. 20483) butenes (butene-1, butene-2, isobutene) Цельностеклянный шприц на (50-100)см3 или газовая пипетка на (250-500)см3 - - не более 5 hours Шприц промывают анализируемым газом 7-10 раз, после этого производят отбор. Газовую пипетку промывают анализируемым воздухом в течение 2-3 мин. со скоростью 0,5-2,0 дм3/мин., равному 7-10 кратному объему, после этого производят отбор перекрывая одновременно оба зажима и выключают аспиратор.
Ethene (ethylene)
Propene (propylene)
C1-C5 (saturated hydrocarb.)
15 FR.1.31.2004.01259 (AUV 0.005.169 MVI) Hexane sorption tube-concentrator (TENAX sorbent) 0,05-0,1 дм3/мин 2 мин 2 недели в холодильни-ке Отбирают последовательно 3 пробы в течение 20 минут.
Decane
Acrolein (acrolein aldehyde, prop-2-en-1-al)
Methylethyl ketone (butane-2-one)
Acetone (propan-2-one)
Hexanone (4-methyl-2-pentanone)
Cyclohexanone
Benzene
Isopropylbenzene (cumene)
O-Xylene (1,2-dimethylbenzene)
M-,P-Xylols (in total)
Styrene (ethenylbenzene)
Toluene (methylbenzene)
Ethylbenzene
FR.1.31.2004.01259 (AUV 0.005.169 MVI) Butan-1-ol sorption tube-concentrator (TENAX sorbent) Of 0.05-0.1 dm3/min 2 min 2 weeks in the refrigerator 3 samples are taken seque
Amyl alcohol (pentanol)
Isobutanol (2-methylpropan-1-ol)
Propyl alcohol (propanol)
Isopentanol (isoamyl alcohol, 3-methyl-1-butanol)
isopropyl alcohol (propan-2-ol)
Ethanol (ethyl alcohol)
Phenol (hydroxybenzene)
Butylacetate
Isoamyl acetate
Vinylacetate (ethenylacetate)
Ethylcellosolve
Ethylacetate
16 PND F 13.1:2:3.25-99 (FR.1.31.2015.20480) C2-C5 (unsaturated) (total); All-glass syringe at (50-100) cm3 or gas pipette at (250-500) cm3 - - no more than 5 hours The syringe is washed with the analyzed gas 7-10 times, after which the selection is made. The gas pipette is washed with the analyzed air for 2-3 minutes. at a speed of 0.5-2.0 dm3 / min, equal to 7-10 times the volume, then the selection is made by simultaneously closing both clips and turning off the aspirator.
C1-C10 (saturated) (total)
Benzene
Toluene
Ethylbenzene
Xylols
Styrene
17 FR. 1. 31. 2011. 11278 (M-16) Formaldehyde Absorption device with a poro 1 dm3/min 20 3 days Glass sampling probe, the spout of which is filled with glass fiber to a height of 10 mm to eliminate the interfering influence of suspended and resinous substances. Sampling is performed simultaneously from two perpendicular holes
18 FR.1.31.2011.11269 (M-24) isocyanates and aromatic amines (aniline, n-nitroaniline, toluylenediisocyanate) 2 series-connected sorption tubes ПВ: 5 dm3/min 20 2 days Sampling probe, the spout of which is filled with glass fiber to a height of 10 mm to eliminate the interfering influence of suspended particles. Sampling is performed simultaneously from two holes (2 sampling lines), 2 series-connected tubes are connected vertically with the sorbent down, the gas current passes through the glass granules from the bottom up.
ATM. vozd.: 5 dm3/min 60 Sampling is carried out simultaneously on 2 lines, in each line there are 2 sequentially connected sorption tubes installed vertically with the sorbent down.
РЗ: 5 dm3/min 15 Sampling is carried out simultaneously on 2 lines, in each line there are 2 sequentially connected sorption tubes installed vertically with the sorbent down.
19 MON F 13.1:2: 3.59-07 (FR.1.31.2013.16458) (M 01-05) aliphatic saturated hydrocarbons of a kerosene fraction C12-C19 disposable carbon type sampler 0.2-0.3 dm3/min 1-3 samples for 20 min selection. consistently 7 days in refrigerator 1-3 samples are taken sequentially for 20 minutes
20 MON F 13.1.56. -07 (FR.1.31.2013.1643) (M-03-06) acetic aldehyde sorption tube-concentrator (TENAX sorbent) 0,1 dm3/min 20 3 days in a freezer Before sampling, a gas-air mixture is drawn from the flue using an aspirator with a volume flow rate of 1 DM / min for 5-10 minutes. Then a sorption tube with the remaining parts of the sampling unit is attached end-to-end to the probe. The sorption tube is placed in a container with snow or finely crushed ice so that its ends remain dry, and the aspirator is turned on. Intensive cooling of the tube is necessary to prevent loss of Acetaldehyde due to overshoot.
butanoic acid
butanoic acid
hexanoic acid
21 MON F 13.1.54-2007 formic acid glass tube with dinochrome n or P sorbent see note see note - Approximate total acid concentration, mg / m3 Sampling rate, dm3 / min Sampling time, min
acetic acid up to 50 5 30
propionic acid 50 to 200 incl 4 25
butanoic acid from 200 to 600 on 3 10
pentanoic acid 600 to 2000 incl 2 5
hexanoic acid


22 PND F 13.1:3.68-09 (FR.1.31.2015.19226) Benzene absorption device with a porous plate 0,5 dm3/min 20 3 days in refrigerator At least 3 samples. Attention: the recommended sampling conditions ensure that the equilibrium concentration of aromatic hydrocarbons in acetic acid is reached at temperatures in the flue or atmospheric air from minus 20° to plus 40°C. Shelf life of samples - 3 days in refrigerator. If it is necessary to store the selected sample for a longer time, the acetic acid concentrate is transferred to a 2 ml glass ampoule and sealed on an alcohol lamp.
Xylene (dimethylbenzene)
23 MON F 13.1.8-97 (FR. 1. 31. 2013. 16439) petrol disposable carbon type sampler (0,1-0,2) dm3 / min Sample volume (0.1-20) dm3 7 days After gas sampling, the VUS samplers are placed in tubes with lapped stoppers and delivered to the laboratory.
Concentration of the substance in gas emissions (mg / m3) Volume of gas emissions sampled (dm3)
from 1 to 10 20
White spirit from 10 to 50 10
from 50 to 500 3-6
Pentanoic acid (valeric) from 500 to 5000 0,3-0,6
from 5000 to 15000 0.1
24 HDPE F 13.1.6-97 Kerosene disposable carbon type sampler (0.1-0.3) dm3 / min Sample volume (0.1-20) dm3 7 days After gas sampling, the VUS samplers are placed in tubes with lapped stoppers and delivered to the laboratory.
Concentration of the substance in gas emissions (mg / m3) Volume of gas emissions sampled (dm3)
from 1 to 10 20
from 10 to 50 10
from 50 to 500 3-6
from 500 to 5000 0,3-0,6
from 5000 to 15000 0.1
25 FR. 1. 31. 2011. 11270 (M-4) Mineral oil (oil aerosol) decontaminated filter blue ribbon 20 dm3 / min 20 7 days Each time, the oil used in this process is selected. Stainless steel sampling tube with replaceable tips. 3-5 samples are taken
26 MON F 13.1.30-02 Turpentine disposable carbon type sampler (0,1-0,3) dm3/min Sample volume (0.1-20) dm3 7 days After gas sampling, the VUS samplers are placed in tubes with lapped stoppers and delivered to the laboratory.
Concentration of the substance in gas emissions (mg / m3) Volume of gas emissions sampled (dm3)
from 1 to 10 20
from 10 to 50 10
from 50 to 500 3-6
from 500 to 5000 0,3-0,6
from 5000 to 15000 0.1
27 MON F 13.1.31-02 Chromium AFA-HP-10; AFA-HP-20; cartridges with fiberglass (10-20) dm3/min sample volume 300 dm3 - -
28 PND F 13.1:2: 3.71-11 (FR.1.31.2015.21767) Aluminum AFA-VP; AFA-HP; AFA-HA (10-15) dm3/min 20 1 month -
Barium
Beryllium
Vanadium
Bismuth
Tungsten
Iron
Gallium
Cadmium
Cobalt
Silicon
Lithium
Magnesium
Manganese
Arsenic
Copper
Molybdenum
Silver
Nikel
Tin
ПНД Ф 13.1:2:3.71-11 (ФР.1.31.2015.21767) Mercury AFA-VP; AFA-HP; AFA-HA (10-15) дм3/мин 20 1 month
Lead
Selenium
Antimony
Titanium
Chromium
Zinc
29 ФР.1.31.2004.01258 (МВИ-М-34-04) Aluminum AFA-VP; AFA-HP; AFA-HA (15-30)dm3 20 1 month -
Барий
Beryllium
Vanadium
Bismuth
Tungsten
Iron
Cadmium
Calcium
Potassium
Cobalt
Silicon
Magnesium
Manganese
Copper
Molybdenum
Arsenic
Натрий
Nikel
Tin
Mercury
Selenium
Lead
Antimony
Titanium
Chromium
Zinc
30 MON F 13.1.76-15 (FR.1.31.2015.20718) (M 06-0-2015) Benz (a)pyrene AFA-VP-20 filters 20 dm3 / min 20 min. - -

Work area air sampling

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№ № RD Name of the characteristic being defined What to sample for Sampling speed Sampling time Shelf life Note
1 ФР.1.31.2001.00384 Углерод (сажа) АФА-ВП-20, АФА-ВП-10 (1-40) dm3/min 20 - -
2 GOST R ISO 16017-1 Acetonitrile sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min - 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
Acrylonitrile (prop-2-isonitrile)
Hexane
Heptane
Decane
Dodecane
Nonane
Octane
Aliphatic saturated hydrocarbons of the gasoline fraction C6-C12
Undecane
Acetone (propan-2-one)
Methylethyl ketone (Butanone)
Hexanon
Diacetone alcohol (4-hydroxy-4-methyl-2-pentanone)
Cyclohexanone
Benzene
Isopropylbenzene (Cumene)
Xylene (dimethylbenzene)
GOST R ISO 16017-1 Pseudocumene (1,2,4-trimethylbenzene) sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min - 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
Styrene (ethenylbenzene)
Toluene (methylbenzene)
Ethylbenzene
Vinyl chloride (chloroethene)
Dichloromethane
1.1-dichloroethylene
Trichloroethane
Trichloroethylene
Carbon tetrachloride (tetrachloromethane)
Chlorobezene
Chloroform (trichloromethane)
Butanol
1.2-dichloroethane
Isobutanol
(2-methylpropan-1-ol)
Метанол (карбинол)
Amyl alcohol (pentanol)
Propyl alcohol (propan-1-ol)
Cyclohexanol (cyclohexyl alcohol)
Ethanol (ethyl alcohol)
Phenol (hydroxybenzene)
Butylacetate
Dibutylphthalate
Dimethylphthalate
Dimethylisophthalate
Diethylphthalate
Isobutylacetate
Methylacetate
Пропилацетат
Vinylacetate (Ethenylacetate)
Ethylacrylate
Ethylacetate
3 ФР.1.31.2011.11272 (М-22) Дивинил (бута-1,3-диен) sorption tube-concentrator (TENAX sorbent) (0,05-0,2) dm3/min 1-3 пробы в течение 15 минут 7 дней в холодильнике -
Benzaldehyde
Methylacetate
Isopropyl acetate (1-methyethyl acetate)
n-propylacetate
isobutylacetate
N-Butylacetate
N-Amylacetate
Isoprene
N-Hexanol
FR.1.31.2011.11272 (M-22) 2-Ethylhexanol sorption tube-concentrator (TENAX sorbent) (0.05-0.2) dm3/min 1-3 samples within 15 minutes 7 days in refrigerator -
Octan-1-ol (n-oktyl alcohol)
Benzyl alcohol (benzyl carbinol)
Propionic acid
Pentanoic acid (valeric)
Hexanoic acid (capronic)
2-ethoxyethyl ether of acetic acid
Methylcellosolve (2-methoxyethanol)
Isopropylalcohol (2-isopropoxyethanol)
Diphenyl ether
Butylcellosolve (2-butoxyethanol)
Durol (1,2,4,5-tetramethylbenzene)
1-methoxypropan-2-ol
1-ethoxypropan-2-ol
4-methylpentan-2-ol
Cyclohexane
Methylbutanoate
Ethylbutanoate
Methylpropionate
Ethylpropionate
Ethylene glycol (1,2-ethanediol)
Propylene glycol (1,2-propanediol)
4 PND F 13.1:2:3.23-98 (FR.1.31.2015. 20483) butenes (butene-1, butene-2, isobutene) syringes 7-10 times pumping the syringe - 5 hours -
Ethene (ethylene)
Propene (propylene)
C1-C5 (saturated hydrocarb.)
5 FR.1.31.2004.01259 (AUV 0.005.169 MVI) Hexane sorption tube-concentrator (TENAX sorbent) 0,05-0,1 dm3/min 2 min 2 weeks in a refrigerator -
Decane
Acrolein (acrolein aldehyde, prop-2-en-1-al)
Methylethyl ketone (butane-2-one)
Acetone (propan-2-one)
Hexanone (4-methyl-2-pentanone)
Cyclohexanone
Benzene
Isopropylbenzene (cumene)
O-Xylene (1,2-dimethylbenzene)
FR.1.31.2004.01259 (AUV 0.005.169 MVI) M-,P-Xylols (in total) sorption tube-concentrator (TENAX sorbent) 0.05-0.1 dm3/min 2 min 2 weeks in a refrigerator -
Styrene (ethenylbenzene)
Toluene (methylbenzene)
Ethylbenzene
Butan-1-ol
Amyl alcohol (pentanol)
Isobutanol (2-methylpropan-1-ol)
Propyl alcohol (propanol)
Isopentanol (isoamyl alcohol, 3-methyl-1-butanol)
isopropyl alcohol (propan-2-ol)
Ethanol (ethyl alcohol)
Phenol (hydroxybenzene)
Butylacetate
Isoamyl acetate
Vinylacetate (ethenylacetate)
Ethylcellosolve
Ethylacetate
6 PND F 13.1:2:3.25-99 (FR.1.31.2015.20480) C2-C5 (unsaturated) (total); syringes 7-10 times pumping the syringe - 5 hours -
C1-C10 (saturated) (total)
Benzene
Toluene
Ethylbenzene
Xylols
Styrene
7 FR.1.31.2011.11269 (M-24) isocyanates and aromatic amines (aniline, n-nitroaniline, toluylenediisocyanate) 2 series-connected sorption tubes ST 412 5 dm3/min 15 2 days in refrigerator 2 sampling lines, each with 2 sequentially connected sorption tubes installed vertically with the sorbent down.
8 PND F 13.1:2: 3.59-07 (FR.1.31.2013.16458) (M 01-05) aliphatic saturated hydrocarbons of a kerosene fraction C12-C19 disposable carbon type sampler 0,2-0,3 dm3/min 15 7 days in refrigerator in the period of 15 minutes 3 consecutive samples are taken
9 MUK 4.1.1957-05 vinyl chloride at the same time on 2 sorption tubes (sorbent Chromosorb 104) 0,2 dm3/min 10 3 days in refrigerator Each air sample is simultaneously sampled into two sorption tubes using 2 samplers.Air is pumped through a narrow opening of the sorption tube, cooled by a refrigerator with ice to 0 °C.
Acetaldehyde
10 MUK 4.1.1143-02 Tiametoxam filter "Sinyaya lenta" 4 dm3/min 5 in a freezer at a temperature of -12 °C for 30 days, in a refrigerator at 4-6 °C - for 7 days. -
11 FR.1.31.2004.01258 (MVI-M-34-04) Aluminum AFA-VP; AFA-HP; AFA-HA 10 dm3/min 15 1 month -
Barium 20 dm3/min 30
Beryllium 20 dm3/min 30
Vanadium 20 dm3/min 30
Bismuth 20 dm3/min 30
Tungsten 20 dm3/min 15
Iron 20 dm3/min 30
Cadmium 20 dm3/min 30
Calcium 20 dm3/min 15
Potassium 20 dm3/min 20
Cobalt 10 dm3/min 15
Silicon 20 dm3/min 15
Magnesium 10 dm3/min 15
Manganese 10 dm3/min 20
Copper 10 dm3/min 15
Molybdenum 20 dm3/min 30
Arsenic 20 dm3/min 30
Натрий 20 dm3/min 20
Nikel 10 dm3/min 20
Tin 20 dm3/min 30
Mercury 20 dm3/min 20
Selenium 20 dm3/min 30
Lead 20 dm3/min 30
Antimony 20 dm3/min 15
Titanium 10 dm3/min 15
Chromium 20 dm3/min 30
Zinc 10 dm3/min 20

Sampling of air in the closed spaces

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№ № RD Name of the characteristic being defined What to sample for Sampling speed Sampling time Shelf life Note
1 GOST R ISO 16000-3 Benzaldehyde (benzoic aldehyde) cartridges with silica-coated DNFH 1 dm3/min 5-60 30 days in a refrigerator, no more than 2 days without a refrigerator -
Dimethyl benzoin aldehyde (2.5-dimethylbenzaldehyde)
Valerian aldehyde (valeraldehyde))
isovalerian aldehyde
hexanal (caproic aldehyde)
croton aldehyde
the propionic aldehyde (propenal)
o-toluene aldehyde
m-toluene aldehyde
p-toluene aldehyde
acetaldehyde (acetic aldehyde)
butanaldehyde (butanal)
formaldehyde (methanal)
acetone (propan-2-one)
2 MUK 4.1.1957-05 vinyl chloride one sample consists of 2 sorption tubes (Chromosorb 104 sorbent) 0,2 dm3/min 10 3 days in refrigerator Air is pumped at a speed of 0.2 dm3/min for 10 minutes through a narrow hole of the sorption tube, cooled by a refrigerator with ice to 0 °C.
Acetaldehyde
3 GOST R ISO 16000-14 PCBs (ind.) sorbent with the applied C13 isotope - - - -
4 MUK 4.1.1044 a-01 Dimethylamine sorbent with the applied C13 isotope 0,2 dm3/min 10 3 days Air is aspirated through a pre-cooled to 0°C outlet of a sorption tube.
Diethylamines
Propylamines
Triethylamines
Ethylamines
Dimethylformamide
5 GOST R ISO 16017-1 Acetonitrile sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min - 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
Acrylonitrile (prop-2-isonitrile)
Hexane
Heptane
Decane
Dodecane
Nonane
Octane
Aliphatic saturated hydrocarbons of the gasoline fraction C6-C12
Undecane
Acetone (propan-2-one)
Methylethyl ketone (Butanone)
Hexanon
Diacetone alcohol (4-hydroxy-4-methyl-2-pentanone)
Cyclohexanone
Benzene
Isopropylbenzene (Cumene)
Xylene (dimethylbenzene)
Pseudocumene (1,2,4-trimethylbenzene)
Styrene (ethenylbenzene)
Toluene (methylbenzene)
Ethylbenzene
Vinyl chloride (chloroethene)
Dichloromethane
1.1-dichloroethylene
Trichloroethane
Trichloroethylene
GOST R ISO 16017-1 Carbon tetrachloride (tetrachloromethane) sorption tube-concentrator (TENAX sorbent) (1-10) dm3/min - 8 hours (or sorption tubes are placed in a clean, uncoated, airtight container. -
Chlorobezene
Chloroform (trichloromethane)
Butanol
1.2-dichloroethane
Isobutanol
(2-methylpropan-1-ol)
Метанол (карбинол)
Amyl alcohol (pentanol)
Propyl alcohol (propan-1-ol)
Cyclohexanol (cyclohexyl alcohol)
Ethanol (ethyl alcohol)
Phenol (hydroxybenzene)
Butylacetate
Dibutylphthalate
Dimethylphthalate
Dimethylisophthalate
Diethylphthalate
Isobutylacetate
Methylacetate
Пропилацетат
Vinylacetate (Ethenylacetate)
Ethylacrylate
Ethylacetate
6 PND F 13.1:2:3.23-98 (FR.1.31.2015. 20483) butenes (butene-1, butene-2, isobutene) syringes 7-10 times pumping the syringe - 5 hours -
Ethene (ethylene)
Propene (propylene)
C1-C5 (saturated hydrocarb.)
7 GOST 17.2.4-05 suspended substances (dust) AFA-VP filter 75 dm3/min At the end of sampling the total volume of air passed is recorded. - -
8 GOST ISO 16000-6 1,2,3-trimethylbenzene sorption tube-concentrator (TENAX sorbent) from 50 to 200 ml3/min from 25 to 100 min 4-weeks from the sampling date -
1,2,4-trimethylbenzene
benzene
Ethylbenzene
Isopropylbenzene
m -, p-Xylenes (sum)
o-xylene
Styrene
Toluene (methylbenzene)
1-butanol
1-pentanol
1-propanol
2-methyl-1-propanol (isobutanol)
cyclohexanol
Phenol (hydroxybenzene)
Acetaldehyde
2-butanone (methylethyl ketone)
acetone
cyclohexanone
1,1,1-trichloroethane
1,1,2-trichloroethane
1,2-dichloroethane
Carbon tetrachloride (tetrachloromethane)
Chlorobezene
Dichloromethane
trichloromethane
tetrachloroethene
trichloroethene
Butylacetate
Ethylacetate
Ethylacrylate
isobutylacrylate
metthyakrylate
methylmethacrylate
Propylacetate
Vinylacetate (Ethenylacetate)
Dibutylphthalate
Dimethylphthalate
hexane
GOST ISO 16000-6 heptane sorption tube-concentrator (TENAX sorbent) from 50 to 200 ml3/min from 25 to 100 min 4-weeks from the sampling date -
octane
nonane
decane
undecane
dodecane
amount of SVOS
amount of VVOC
TVOC in toluene equivalent
Sampling for all types of air
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